Chemistry 3022 - Organic Chemistry Laboratory Materials

    The following table provides important information needed for this course and links to other documents you will need.  Note that you should prepare for the experiments in the order provided below and the DUE DATES are provided as they are assigned.  You must manage your own schedule in completing the labs in a timely manner.  No time will be permitted outside of your normal lab time to work in the lab.  Everyone is working under the same time constraints, so plan ahead and be ready to work in lab.  It is expected that you will work on several labs simultaneously (multi-tasking) in this course.
    Be sure to come to lab on Thursday, Sept. 2, 1999 ready to work on the "Structures from Spectra (Lab #1).  You should read and work through all the material for Lab #1 and obtain print-outs as requested in that lab write-up.

Check out this link for help with your spectroscopic data: IR & NMR database

IT'S AMINO WORLD WITHOUT ORGANIC CHEMISTRY _____________________________________________ What's the best vitamin for making friends? ___________________________________________________ B-1_____________________________________________Two atoms are walking together. One atom says to the other, "I think I've lost an electron." The other responds,"Are you sure?" The first replies, "I'm positive!"

Lab Experiments Topic   Due Dates
Thurs. Lab
1 a) Read Syllabus
b) Read Additional Common Practices
c) Prepare notebook & Table of Contents
d) Structures from Spectra
   
2 Nitration of Halobenzenes and Thin Layer Chromatography    
3 Grignard Synthesis of Benzoic Acid   Friday
10/8/99
5:00 pm
4

a) Two Component Unknown Mixture Separation by Extraction
b) Extraction Diagram
c) Identification of Acids, Bases and Neutral Compounds

*Review from CHEM 3012:  Separation of a Known 3 Component Mixture by Extraction

   
5 Dissociation Constants of Acids   Wed.
11/24/99
noon
6 Column Chromatography of the Fluorene Oxidation Reaction    
7 The Chemistry of Esters    
8 Preparation of Hydroxyacetanilide